Nanocrystal synthesis is a fun, provided you are good at it.
If it is monodispersed in size, the color is pure and it looks beautifully organized in TEM images. It is simply stunning. However, it may take time to
master the skills. You need to improve your skill day by day, sharpen your
sense, and make your own tips. Those who do nanocrystal synthesis are craftsmen
who are proud of their skill.
Interestingly, some have good hands to synthesize things. Some do not. You cannot
rely only on your friends’ tips, because the way you handle chemicals is
different from the way your friend handles them. However, you can rely on one
thing….. science!
There are tons of research papers, so I picked up 5 papers that have been well read in the field. These papers might be a good starting point. Take heed of their advice and adjust your
work accordingly.
successfully synthesized nanocrystals |
5 Basic
classic papers on nanocrystal synthesis you need to know
Nucleation and growth
Lamer, V. K.; Dinegar, R. H. J. Am. Chem. Soc. 1950, 72,4847.
Murray, C. B.; Kagan, C. R.; Bawendi, M. G. Ann. Rev. Mater.Soc. 2000,30, 545.
Basic Characterization
Murray, C. B.; Norris, D. J.; Bawendi, M. G. J. Am. Chem.Soc. 1993, 115, 8706.
Anisotropic nanocrystal synthesis
Yin, Y.; Alivisatos, A. P. Nature 2005, 437, 664
X. Peng.; Alivisatos, AP et al Nature 2000 404, 59 .
Good luck on being a master of nanocrystal synthesis!